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| Title: | A new method for compound-specific stable chlorine isotope analysis basics and application |
|---|---|
| From: |
von Kaori Sakaguchi-Söder. [Hrsg.: Verein zur Förderung des Instituts IWAR der TU Darmstadt e.V.]
|
| Person: |
Sakaguchi-Söder, Kaori
Verfasser aut |
| Main Author: | |
| Format: | Thesis Book |
| Language: | English |
| Published: |
Darmstadt
Inst. IWAR
2010
|
| Series: | Schriftenreihe IWAR
209 |
| Subjects: | |
| Online Access: | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022485884&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| Item Description: | Literaturverz. S. 181 - 188 |
| Physical Description: | XXII, 188 S. Ill., graph. Darst. 21 cm |
| ISBN: | 9783940897053 |
Staff View
MARC
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| 100 | 1 | |a Sakaguchi-Söder, Kaori |e Verfasser |0 (DE-588)143374516 |4 aut | |
| 245 | 1 | 0 | |a A new method for compound-specific stable chlorine isotope analysis |b basics and application |c von Kaori Sakaguchi-Söder. [Hrsg.: Verein zur Förderung des Instituts IWAR der TU Darmstadt e.V.] |
| 264 | 1 | |a Darmstadt |b Inst. IWAR |c 2010 | |
| 300 | |a XXII, 188 S. |b Ill., graph. Darst. |c 21 cm | ||
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| 490 | 1 | |a Schriftenreihe IWAR |v 209 | |
| 500 | |a Literaturverz. S. 181 - 188 | ||
| 502 | |a Zugl.: Darmstadt, Techn. Univ., Diss., 2010 | ||
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Record in the Search Index
| DE-BY-TUM_call_number | 0001 2023 A 1375 |
|---|---|
| DE-BY-TUM_katkey | 2721265 |
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| adam_text |
TABLE
OF
CONTENTS
TABLE
OF
CONTENTS
ACKNOWLEDGEMENTS
.
I
EXECUTIVE
SUMMARY
.
III
KURZZUSAMMENFASSUNG
.
V
TABLE
OF
CONTENTS
.VII
LIST
OF
FIGURES
.
XI
LIST
OF
TABLES
.
XV
ABBREVIATIONS
AND
CONVENTIONS
ADOPTED
FOR
THIS
THESIS
.XIX
1.
INTRODUCTION
.
1
1.1.
BACKGROUND
.
1
1.2.
AIM
OF
THE
DOCTORAL
WORK
.
2
1.3.
NOVELTIES
OF
THE
DOCTORAL
WORK
.
4
1.4.
SIGNIFICANCE
OF
THE
DOCTORAL
WORK
.
4
BASICS
OF
COMPOUND-SPECIFIC
STABLE
ISOTOPE
ANALYSIS
(CSIA)
2.
STABLE
ISOTOPE
ANALYSES
.
7
2.1.
INTRODUCTION
.
7
2.2.
STABLE
ISOTOPES
.
8
2.3.
STABLE
ISOTOPE
FRACTIONATION
.
10
2.4.
STABLE
ISOTOPE
FRACTIONATION
FACTOR/ENRICHMENT
FACTOR
.
13
2.5.
APPLICATION
OF
CSIA
TO
INVESTIGATE
BIODEGRADATION/CHEMICAL
TRANSPORTATION
.
14
3.
AVAILABLE
TECHNIQUES
FOR
STABLE
CHLORINE
ISOTOPE
ANALYSIS
.
17
3.1.
INTRODUCTION
.
17
3.2.
OFF-LINE
DI-IRMS
METHODS
.
17
3.3.
TIMS
METHOD
.
22
3.3.1.
STABLE
CHLORINE
ISOTOPE
ANALYSIS
FOR
CHLORINATED
ETHENES
AND
ETHANES
USING
TIMS.
23
3.3.2.
STABLE
CHLORINE
ISOTOPE
ANALYSIS
FOR
DIOXINS
(OCDD)
USING
TIMS
.
24
3.4.
ONLINE
METHODS
FOR
C1-CSIA
.
25
3.5.
PRACTICABILITY
AND
LIMITATION
OF
AVAILABLE
METHODS
.
26
3.5.1.
SENSITIVITY
AND
PRECISION
.
26
3.5.2.
LIMITATIONS
OF
AVAILABLE
METHODS
.
28
TABLE
OF
CONTENTS
DEVELOPING
A
NEW
METHOD
FOR
COMPOUND-SPECIFIC
STABLE
CHLORINE
ISOTOPE
ANALYSIS
4.
DEVELOPING
A
NEW
METHOD
FOR
C1-CSIA
.
33
4.1.
INTRODUCTION
.
33
4.2.
BASICS
OF
QUADRUPOLE
GC/MS
.
34
4.2.1.
FUNCTION
OF
GC/MS
.
34
4.2.2.
GAS
CHROMATOGRAPHY
(GC)
.
35
4.2.3.
QUADRUPOLE
MASS
SPECTROMETRY
(MS)
.37
4.3.
THEORY
OF
DETERMINING
THE
PROBABILITY
OF
OCCURRENCE
OF
ISOTOPOLOGUES
.
40
4.4.
THEORY
OF
DETERMINING
THE
NUMBER
OF
ISOTOPOLOGUES
AND
THE
NUMBER
OF
ISOTOPOMERS
.42
4.4.1.
THE
NUMBER
OF
ISOTOPOLOGUES
.42
4.4.2.
IDENTIFYING
ALL
STOCHASTICALLY
POSSIBLE
ISOTOPIC
COMBINATIONS
.
44
4.5.
EXAMPLE:
DETERMINING
THE
NUMBER
OF
ISOTOPOLOGUES
AND
ISOTOPOMERS
OF
PCE
.46
4.6.
EXAMPLE:
DETERMINING
THE
PROBABILITY
OF
OCCURRENCE
OF
PCE
ISOTOPOLOGUES
.
48
4.7.
BASIC
CONCEPT
OF
DEVELOPING
A
NEW
DATA
ANALYSIS
METHOD
FOR
CSIA
FOR
THE
USE
OF
QUADRUPOLE
GC/MS
.
51
4.7.1. DETERMINING
THE
CHLORINE
ISOTOPE
RATIO
USING
PEAK
INTENSITIES
OF
MOLECULAR
IONS.
51
4.7.2.
SELECTING
THE
MOST
APPROPRIATE
PEAKS
FOR
SENSITIVE
AND
ACCURATE
C1-CSIA
USING
QUADRUPOLE
GC/MS
.54
4.7.3. DETERMINING
THE
CHLORINE
ISOTOPE
RATIO
USING
PEAK
INTENSITIES
OF
FRAGMENT
IONS
.
57
5.
DEVELOPING
MATHEMATICAL
EQUATIONS
FOR
DETERMINING
CHLORINE
ISOTOPE
RATIOS
OF
SELECTED
CHLORINATED
COMPOUNDS
.
61
5.1.
INTRODUCTION
.
61
5.2.
MATHEMATICAL
EQUATIONS
FOR
CHLORINATED
ETHENES
.
63
5.2.1.
PCE
.
63
5.2.2.
TCE
.
66
5.2.3.
DCE-ISOMERS
.
69
5.2.4.
VC
.
73
5.3.
MATHEMATICAL
EQUATIONS
FOR
CHLORINATED
ETHANES
.
75
5.3.1.
1,1,1-TCA
.
75
5.3.2.
DCA
ISOMERS
.
78
5.4.
MATHEMATICAL
EQUATION
FOR
A
CHLORINATED
HERBICIDE,
ATRAZINE
.
83
5.5.
MATHEMATICAL
EQUATIONS
FOR
DIOXINS
.86
5.5.1. OCTACHLORODIBENZO-P-DIOXIN
(OCDD)
.
.86
5.5.2.
TETRACHLORODIBENZO-P-DIOXIN
(TECDD)
.
90
5.6.
SUMMARY
AND
CONCLUSION
OF
CHAPTER
5
.
92
VIII
TABLE
OF
CONTENTS
APPLICATION
OF
THE
NEW
METHOD
6.
PRACTICABILITY
OF
THE
METHOD
FOR
GAS-PHASE
ANALYSIS
ON
CHLORINATED
ETHENES
.
97
6.1.
INTRODUCTION
.
97
6.2.
EXPERIMENTAL
PROCEDURE
.
97
6.3.
RESULTS
.
99
6.3.1.
COMPOUND-SPECIFIC
CAPABILITY
AND
REPRODUCIBILITY
OF
THE
METHOD
.
99
6.3.2.
INFLUENCE
OF
MS
SOURCE
TEMPERATURES
ON
DELTA
VALUES
.
101
6.3.3.
INFLUENCE
OF
SPLIT
RATIOS
ON
DELTA
VALUES
.
105
6.3.4.
INFLUENCE
OF
INJECTED
MASSES
ON
DELTA
VALUES
.
109
6.4.
SUMMARY
AND
CONCLUSION
OF
CHAPTER
6
.
113
7.
INFLUENCE
OF
INJECTED
MASSES
ON
DELTA
VALUES:
MANUAL
HEADSPACE
ANALYSIS
.
115
7.1.
INTRODUCTION
.
115
7.2.
EXPERIMENTAL
PROCEDURE
.
116
7.2.1.
PREPARATION
FOR
SELECTING
AN
IN-HOUSE
REFERENCE
SUBSTANCE
.
116
7.2.2.
PREPARATION
OF
HEADSPACE
SAMPLES
FOR
PCE,
TCE,
CIS-DCE,
TRANS-DCE,
AND
VC.
117
7.2.3.
GC/MS
CONDITIONS
.
119
7.3.
RESULTS
.
120
7.3.1.
SELECTING
AN
IN-HOUSE
REFERENCE
SUBSTANCE
.
120
7.3.2.
INFLUENCE
OF
INJECTED
MASS
ON
DELTA
VALUE
.
124
7.3.3.
INFLUENCE
OF
INJECTED
MASSES
ON
THE
INTERNAL
PRECISION
IN
DETERMINING
DELTA
VALUESL34
7.4.
SUMMARY
AND
CONCLUSION
OF
CHAPTER
7
.
140
8.
FEASIBILITY
OF
THE
NEW
METHOD
TO
DERIVE
CHLORINE
ISOTOPE
FRACTIONATION
FACTORS
.
143
8.1.
INTRODUCTION
.
143
8.2.
REDUCTIVE
DECHLORINATION
OF
TCE
USING
ZERO-VALENT
IRON
AND
IRON
SULFIDE
.
143
8.3.
EXPERIMENTAL
PROCEDURE
.
144
8.3.1.
ABIOTIC
REDUCTIVE
DECHLORINATION
OF
TCE
USING
ZERO-VALENT
IRON
.
144
8.3.2.
ABIOTIC
REDUCTIVE
DECHLORINATION
OF
TCE
USING
FES
.
145
8.3.3.
GC/MS
CONDITIONS
FOR
THE
C1-CSIA
.
146
8.3.4.
CALCULATION
FOR
DELTA
VALUES
.
146
8.4.
RESULTS
.
146
8.4.1.
DETERMINING
A-VALUE
DURING
THE
REDUCTIVE
DECHLORINATION
OF
TCE
USING
ZERO-VALENT
IRON
.
146
8.4.2.
DETERMINING
A-VALUE
DURING
THE
REDUCTIVE
DECHLORINATION
OF
TCE
USING
FES
.
151
8.5.
SUMMARY
AND
CONCLUSION
OF
CHAPTER
8
.
154
IX
TABLE
OF
CONTENTS
9.
CL-CSIA
USING
PURGE
AND
TRAP
.
157
9.1.
INTRODUCTION
.
157
9.2.
EXPERIMENTAL
PROCEDURE
.
157
9.2.1.
PREPARATION
OF
CAH
STANDARDS
AND
AN
IN-HOUSE
REFERENCE
.
157
9.2.2.
P&T-GC/MS
SETTINGS
.
158
9.3.
RESULTS
.
159
9.3.1.
PRECISION
OF
THE
GC/MS
METHOD
USING
P&T
SYSTEM
.
159
9.3.2.
PEAK
AREA
DEPENDENCY
OF
THE
GC/MS
METHOD
.
161
9.3.3. MANUAL
ANALYSIS
VERSUS
P&T
ANALYSIS
.
166
9.4.
SUMMARY
AND
CONCLUSION
FOR
CHAPTER
9
.
170
SUMMARY,
OUTLOOK,
AND
RECOMMENDATIONS
10.
SUMMARY
AND
OUTLOOK
.
175
11.
RECOMMENDATIONS
.
179
BIBLIOGRAPHY
.
181
X |
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| dewey-raw | 539.723 |
| dewey-search | 539.723 |
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| dewey-tens | 530 - Physics |
| discipline | Chemie / Pharmazie Physik Allgemeines |
| format | Thesis Book |
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| genre_facet | Hochschulschrift |
| id | DE-604.BV037332000 |
| illustrated | Illustrated |
| indexdate | 2025-03-04T07:00:14Z |
| institution | BVB |
| isbn | 9783940897053 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-022485884 |
| oclc_num | 710976831 |
| open_access_boolean | |
| owner | DE-83 DE-91 DE-BY-TUM DE-M490 |
| owner_facet | DE-83 DE-91 DE-BY-TUM DE-M490 |
| physical | XXII, 188 S. Ill., graph. Darst. 21 cm |
| publishDate | 2010 |
| publishDateSearch | 2010 |
| publishDateSort | 2010 |
| publisher | Inst. IWAR |
| record_format | marc |
| series | Schriftenreihe IWAR |
| series2 | Schriftenreihe IWAR |
| spellingShingle | Sakaguchi-Söder, Kaori A new method for compound-specific stable chlorine isotope analysis basics and application Schriftenreihe IWAR Isotopenhäufigkeit (DE-588)4162584-5 gnd Chlorverbindungen (DE-588)4147848-4 gnd |
| subject_GND | (DE-588)4162584-5 (DE-588)4147848-4 (DE-588)4113937-9 |
| title | A new method for compound-specific stable chlorine isotope analysis basics and application |
| title_auth | A new method for compound-specific stable chlorine isotope analysis basics and application |
| title_exact_search | A new method for compound-specific stable chlorine isotope analysis basics and application |
| title_full | A new method for compound-specific stable chlorine isotope analysis basics and application von Kaori Sakaguchi-Söder. [Hrsg.: Verein zur Förderung des Instituts IWAR der TU Darmstadt e.V.] |
| title_fullStr | A new method for compound-specific stable chlorine isotope analysis basics and application von Kaori Sakaguchi-Söder. [Hrsg.: Verein zur Förderung des Instituts IWAR der TU Darmstadt e.V.] |
| title_full_unstemmed | A new method for compound-specific stable chlorine isotope analysis basics and application von Kaori Sakaguchi-Söder. [Hrsg.: Verein zur Förderung des Instituts IWAR der TU Darmstadt e.V.] |
| title_short | A new method for compound-specific stable chlorine isotope analysis |
| title_sort | a new method for compound specific stable chlorine isotope analysis basics and application |
| title_sub | basics and application |
| topic | Isotopenhäufigkeit (DE-588)4162584-5 gnd Chlorverbindungen (DE-588)4147848-4 gnd |
| topic_facet | Isotopenhäufigkeit Chlorverbindungen Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022485884&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV037413929 |
| work_keys_str_mv | AT sakaguchisoderkaori anewmethodforcompoundspecificstablechlorineisotopeanalysisbasicsandapplication |