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Titel:	50 and more essential NMR experiments a detailed guide
Weiterer Titel:	Fifty and more essential NMR experiments
Von:	Matthias Findeisen ; Stefan Berger
Person:	Findeisen, Matthias Verfasser aut Berger, Stefan 1946-2023
Hauptverfassende:	Findeisen, Matthias (VerfasserIn), Berger, Stefan 1946-2023 (VerfasserIn)
Format:	Buch
Sprache:	Englisch
Veröffentlicht:	Weinheim Wiley-VCH 2014
Schlagworte:	Experiment NMR-Spektroskopie
Online-Zugang:	http://deposit.dnb.de/cgi-bin/dokserv?id=4329655&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026119778&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
Beschreibung:	308 S. Ill., graph. Darst.
ISBN:	9783527334834

Internformat

MARC


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Datensatz im Suchindex

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DE-BY-UBR_location	UB Lesesaal Chemie / Pharmazie
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adam_text	IMAGE 1 CONTENTS PREFACE CHAPTER 1 THE ORGANIC SET OF NMR SPECTRA 1 1.1 THE H NMR EXPERIMENT 3 1.2 APT- I3 C NMR 7 1.3 COSY 11 1.4 NOESY 17 1.5 HSQC 23 1.6 HMBC 29 CHAPTER 2 ADVANCED ORGANIC NMR SPECTROSCOPY 35 2.1 2D ./-RESOLVED H NMR SPECTROSCOPY 37 2.2 ROESY 41 2.3 TOCSY 45 2.4 HSQC-TOCSY 49 2.5 HOESY 53 2.6 INADEQUATE 57 2.7 ADEQUATE 61 2.8 J-HMBC 65 2.9 GATED DECOUPLING 71 CHAPTER 3 SELECTIVE METHODS 75 3.1 WATER SUPPRESSION BY PRESATURATION 77 3.2 SOLVENT SUPPRESSION BY 1D-NOESY 81 3.3 WATER SUPPRESSION BY SOGGY EXCITATION SCULPTING 85 3.4 SOLVENT SUPPRESSION USING WET 89 3.5 SELTOCSY 93 3.6 SELNOESY 97 3.7 SELINCOR 101 3.8 SELINQUATE 105 3.9 BAND SELECTIVE HMBC 109 CHAPTER 4 HETERONUCLEAR NMR 113 4.1 B NMR SPECTROSCOPY 119 4.2 L5 N NMR SPECTROSCOPY 123 4.3 L7 0 NMR SPECTROSCOPY 127 4.4 L9 F NMR SPECTROSCOPY 131 4.5 29 SI NMR SPECTROSCOPY 135 4.6 57 FE NMR SPECTROSCOPY 139 4.7 L95 PT NMR SPECTROSCOPY 145 HTTP://D-NB.INFO/1034511149 IMAGE 2 CHAPTER S EXPERIMENTS IN PHYSICAL ORGANIC CHEMISTRY 149 5.1 MEASUREMENT OF THE SPIN-LATTICE RELAXATION TIME T T 151 5.2 MEASUREMENT OF THE SPIN-SPIN RELAXATION TIME T 2 155 5.3 DYNAMIC H NMR SPECTROSCOPY 159 5.4 DIFFUSION MEASUREMENT WITH DOSY 163 5.5 RESIDUAL DIPOLAR COUPLINGS (RDC) 167 CHAPTER 6 ORGANIC CHEMISTRY APPLICATIONS 173 6.1ASIS 175 6.2 CHIRALITY DETERMINATION 179 6.3 ADVANCED MOSHER METHOD 183 6.4 QUANTITATIVE NMR AND RELAXATION REAGENTS 187 6.5 DETERMINATION OF ASSOCIATION CONSTANTS K 193 6.6 STD NMR 199 6.7 A KINETIC EXPERIMENT 203 CHAPTER 7 AN EXCURSION TO THE SOLID STATE AND TO STRUCTURAL BIOLOGY 209 7.1 THE CP/MAS EXPERIMENT 211 7.2 HIGH-RESOLUTION MAGIC-ANGLE SPINNING 215 7.3 HN-HSQC 219 7.4 HNCA 225 CHAPTER 8 MAINTENANCE AND CALIBRATION 233 8.1 CALIBRATION OF PULSE DURATION IN THE TRANSMITTER CHANNEL 235 8.2 CALIBRATION OF THE PULSE DURATION IN THE INDIRECT CHANNEL 241 8.3 SHAPED PULSES 247 8.4 ADIABATIC PULSES 253 8.5 TEMPERATURE CALIBRATION IN NMR 257 8.6 CALIBRATION OF PULSED FIELD GRADIENTS 265 APPENDIX ANSWERS 273 PULSE PROGRAMS 295 ELEMENTARY PRODUCT OPERATOR FORMALISM RULES 296 CHEMICAL SHIFT AND SPIN-COUPLING DATA FOR STRYCHNINE 298 PICTURE CREDITS 300 INDEX 301
any_adam_object	1
author	Findeisen, Matthias Berger, Stefan 1946-2023
author_GND	(DE-588)124698107
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ctrlnum	(OCoLC)862797517 (DE-599)DNB1034511149
dewey-full	543.66
dewey-hundreds	500 - Natural sciences and mathematics
dewey-ones	543 - Analytical chemistry
dewey-raw	543.66
dewey-search	543.66
dewey-sort	3543.66
dewey-tens	540 - Chemistry and allied sciences
discipline	Chemie / Pharmazie
format	Book
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indexdate	2024-12-20T16:31:45Z
institution	BVB
isbn	9783527334834
language	English
oai_aleph_id	oai:aleph.bib-bvb.de:BVB01-026119778
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physical	308 S. Ill., graph. Darst.
publishDate	2014
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record_format	marc
spellingShingle	Findeisen, Matthias Berger, Stefan 1946-2023 50 and more essential NMR experiments a detailed guide Experiment (DE-588)4015999-1 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd
subject_GND	(DE-588)4015999-1 (DE-588)4075421-2
title	50 and more essential NMR experiments a detailed guide
title_alt	Fifty and more essential NMR experiments
title_auth	50 and more essential NMR experiments a detailed guide
title_exact_search	50 and more essential NMR experiments a detailed guide
title_full	50 and more essential NMR experiments a detailed guide Matthias Findeisen ; Stefan Berger
title_fullStr	50 and more essential NMR experiments a detailed guide Matthias Findeisen ; Stefan Berger
title_full_unstemmed	50 and more essential NMR experiments a detailed guide Matthias Findeisen ; Stefan Berger
title_short	50 and more essential NMR experiments
title_sort	50 and more essential nmr experiments a detailed guide
title_sub	a detailed guide
topic	Experiment (DE-588)4015999-1 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd
topic_facet	Experiment NMR-Spektroskopie
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